Information card for entry 7103872

Structure parameters

• Formula: C66 H68 B F24 N3 P2 Pd
• Calculated formula: C66 H68 B F24 N3 P2 Pd
• Title of publication: A five coordinate PdII complex stable in solution and in the solid state
• Authors of publication: Martin Broring; Carsten D. Brandt
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2003
• a: 14.5341 ± 0.0011 Å
• b: 15.1714 ± 0.0011 Å
• c: 17.1442 ± 0.0012 Å
• α: 95.971 ± 0.001°
• β: 97.231 ± 0.001°
• γ: 105.826 ± 0.001°
• Cell volume: 3570 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0996
• Weighted residual factors for all reflections included in the refinement: 0.1012
• Goodness-of-fit parameter for all reflections included in the refinement: 1.143
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No