Information card for entry 7103873

Structure parameters

• Formula: C63 H59 B F24 N3 P Pd
• Calculated formula: C63 H59 B F24 N3 P Pd
• Title of publication: A five coordinate PdII complex stable in solution and in the solid state
• Authors of publication: Martin Broring; Carsten D. Brandt
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2003
• a: 12.9944 ± 0.0011 Å
• b: 20.5527 ± 0.0017 Å
• c: 25.0962 ± 0.0021 Å
• α: 90°
• β: 104.331 ± 0.001°
• γ: 90°
• Cell volume: 6493.9 ± 0.9 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0868
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1347
• Weighted residual factors for all reflections included in the refinement: 0.1456
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No