Information card for entry 7104098

Structure parameters

• Formula: C50 H59 As Cl2 N2 P
• Calculated formula: C50 H59 As Cl2 N2 P
• Title of publication: Inhibited chelation in the new γ-phosphino-β-diketiminate to give phosphine → arsine coordination
• Authors of publication: Ragogna, Paul J.; Burford, Neil; D'eon, Mark; McDonald, R.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1052 - 1053
• a: 11.4457 ± 0.0009 Å
• b: 12.4619 ± 0.001 Å
• c: 16.9019 ± 0.0013 Å
• α: 94.92 ± 0.002°
• β: 104.742 ± 0.001°
• γ: 90.251 ± 0.002°
• Cell volume: 2322 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0949
• Weighted residual factors for all reflections included in the refinement: 0.101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No