Information card for entry 7104413

Structure parameters

• Formula: C46 H65 Ge2 N3
• Calculated formula: C46 H65 Ge2 N3
• SMILES: [Ge]1([N](=C(C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C)[Ge]1[N](=C(C=C1C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: An unsymmetric substituted digermylene with a Ge(I)-Ge(I) bond and synthesis of a germylene-stannylene with a Ge(I)-Sn(I) bond.
• Authors of publication: Wang, Wenyuan; Inoue, Shigeyoshi; Yao, Shenglai; Driess, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 19
• Pages of publication: 2661 - 2663
• a: 44.536 ± 0.002 Å
• b: 9.8204 ± 0.0005 Å
• c: 21.8135 ± 0.001 Å
• α: 90°
• β: 116.03 ± 0.004°
• γ: 90°
• Cell volume: 8572.7 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1461
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.0777
• Weighted residual factors for all reflections included in the refinement: 0.0965
• Goodness-of-fit parameter for all reflections included in the refinement: 0.917
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No