Information card for entry 7104414

Structure parameters

• Formula: C46 H65 Ge N3 Sn
• Calculated formula: C46 H65 Ge N3 Sn
• Title of publication: An unsymmetric substituted digermylene with a Ge(I)-Ge(I) bond and synthesis of a germylene-stannylene with a Ge(I)-Sn(I) bond.
• Authors of publication: Wang, Wenyuan; Inoue, Shigeyoshi; Yao, Shenglai; Driess, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 19
• Pages of publication: 2661 - 2663
• a: 8.6778 ± 0.0001 Å
• b: 12.0514 ± 0.0004 Å
• c: 21.0797 ± 0.0006 Å
• α: 96.333 ± 0.002°
• β: 97.393 ± 0.002°
• γ: 99.141 ± 0.002°
• Cell volume: 2139.08 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0707
• Weighted residual factors for all reflections included in the refinement: 0.0734
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No