Information card for entry 7104671

Structure parameters

• Formula: C88 H98 Ge2 O6
• Calculated formula: C88 H98 Ge2 O6
• Title of publication: An isolable o-quinodimethane and its fixation of molecular oxygen to give an endoperoxide.
• Authors of publication: Ghereg, Dumitru; Ech-Cherif El Kettani, Sakina; Lazraq, Mohamed; Ranaivonjatovo, Henri; Schoeller, Wolfgang W; Escudié, Jean; Gornitzka, Heinz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 32
• Pages of publication: 4821 - 4823
• a: 14.7436 ± 0.001 Å
• b: 17.0689 ± 0.0011 Å
• c: 17.6474 ± 0.0011 Å
• α: 67.084 ± 0.001°
• β: 66.935 ± 0.001°
• γ: 67.844 ± 0.001°
• Cell volume: 3629 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0982
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1139
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No