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Information card for entry 7104672
Preview
Coordinates | 7104672.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C74 H71 Ge2 O2.5 |
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Calculated formula | C74 H71 Ge2 O2.5 |
Title of publication | An isolable o-quinodimethane and its fixation of molecular oxygen to give an endoperoxide. |
Authors of publication | Ghereg, Dumitru; Ech-Cherif El Kettani, Sakina; Lazraq, Mohamed; Ranaivonjatovo, Henri; Schoeller, Wolfgang W; Escudié, Jean; Gornitzka, Heinz |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2009 |
Journal volume | 34 |
Journal issue | 32 |
Pages of publication | 4821 - 4823 |
a | 10.5043 ± 0.0009 Å |
b | 21.2079 ± 0.0019 Å |
c | 26.522 ± 0.002 Å |
α | 90° |
β | 95.893 ± 0.002° |
γ | 90° |
Cell volume | 5877.2 ± 0.9 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.172 |
Residual factor for significantly intense reflections | 0.0868 |
Weighted residual factors for significantly intense reflections | 0.1668 |
Weighted residual factors for all reflections included in the refinement | 0.1976 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7104672.html
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