Information card for entry 7104781

Structure parameters

• Common name: Sym-anti perchlorato
• Chemical name: Sym-anti perchlorato
• Formula: C14 H29 Cl2 Co N4 O8
• Calculated formula: C14 H29 Cl2 Co N4 O8
• Title of publication: The first structurally characterised perchlorato-cobalt(III) complexes, involving the C-bonded macrobicyclic ligand 1,4,8,11-tetraazabicyclo[9.5.2]octadecane
• Authors of publication: Zhou, Xiangting; Day, Anthony I.; Willis, Anthony C.; Jackson, W. Gregory
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2386 - 2387
• a: 8.1097 ± 0.0001 Å
• b: 14.6807 ± 0.0003 Å
• c: 8.7957 ± 0.0002 Å
• α: 90°
• β: 108.442 ± 0.001°
• γ: 90°
• Cell volume: 993.4 ± 0.03 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for all reflections included in the refinement: 0.0416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0641
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No