Information card for entry 7104782

Structure parameters

• Formula: C74 H85 Br Mg O5 Pb4
• Calculated formula: C74 H85 Br Mg O5 Pb4
• Title of publication: Tris(triphenylplumbyl)plumbate: an anion with three stretched lead‒lead bonds
• Authors of publication: Stabenow, Frank; Saak, Wolfang; Weidenbruch, Manfred
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2342 - 2343
• a: 15.699 ± 0.0004 Å
• b: 14.1672 ± 0.0005 Å
• c: 32.0448 ± 0.0007 Å
• α: 90°
• β: 95.009 ± 0.003°
• γ: 90°
• Cell volume: 7099.9 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0855
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0657
• Weighted residual factors for all reflections included in the refinement: 0.0748
• Goodness-of-fit parameter for all reflections included in the refinement: 0.835
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No