Information card for entry 7105136

Structure parameters

• Common name: 2,6-Bis(dimethoxyphosphoryl)-1,2,3,4-tetrahydroquinoline
• Chemical name: 2,6-Bis(dimethoxyphosphoryl)-1,2,3,4-tetrahydroquinoline
• Formula: C13 H20 N2 O8 P2
• Calculated formula: C12.999 H19.997 N2 O8 P2
• Title of publication: One-pot tandem 1,4-1,2-addition of phosphites to quinolines.
• Authors of publication: De Blieck, Ann; Masschelein, Kurt G R; Dhaene, Fréderic; Rozycka-Sokolowska, Ewa; Marciniak, Bernard; Drabowicz, Jozef; Stevens, Christian V
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 46
• Journal issue: 2
• Pages of publication: 258 - 260
• a: 10.0124 ± 0.0004 Å
• b: 10.3614 ± 0.0005 Å
• c: 10.4335 ± 0.0004 Å
• α: 63.537 ± 0.004°
• β: 80.792 ± 0.003°
• γ: 67.351 ± 0.004°
• Cell volume: 894.17 ± 0.07 ų
• Cell temperature: 292 ± 2 K
• Ambient diffraction temperature: 292 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.1309
• Weighted residual factors for all reflections included in the refinement: 0.1463
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No