Crystallography Open Database

Information card for entry 7105527

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Coordinates	7105527.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H51 B3 F24 N2 P Rh
Calculated formula	C47 H51 B3 F24 N2 P Rh
Title of publication	Amino-borane oligomers bound to a Rh(i) metal fragment
Authors of publication	Dallanegra, Romaeo; Chaplin, Adrian B.; Tsim, Jennifer; Weller, Andrew S.
Journal of publication	Chemical Communications
Year of publication	2010
Journal volume	46
Journal issue	18
Pages of publication	3092 - 3094
a	13.1134 ± 0.0001 Å
b	15.0932 ± 0.0001 Å
c	15.6507 ± 0.0002 Å
α	84.6142 ± 0.0004°
β	78.4318 ± 0.0004°
γ	86.9282 ± 0.0004°
Cell volume	3019.4 ± 0.05 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0549
Residual factor for significantly intense reflections	0.0466
Weighted residual factors for significantly intense reflections	0.1304
Weighted residual factors for all reflections included in the refinement	0.1364
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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