Information card for entry 7105528

Structure parameters

• Formula: C48.5 H57 B4 F24 N3 P Rh
• Calculated formula: C48.5 H57 B4 F24 N3 P Rh
• Title of publication: Amino-borane oligomers bound to a Rh(i) metal fragment
• Authors of publication: Dallanegra, Romaeo; Chaplin, Adrian B.; Tsim, Jennifer; Weller, Andrew S.
• Journal of publication: Chemical Communications
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 18
• Pages of publication: 3092 - 3094
• a: 13.2206 ± 0.0001 Å
• b: 18.3347 ± 0.0001 Å
• c: 24.0722 ± 0.0002 Å
• α: 90°
• β: 98.7365 ± 0.0004°
• γ: 90°
• Cell volume: 5767.3 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.1055
• Weighted residual factors for all reflections included in the refinement: 0.1143
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No