Information card for entry 7105921

Structure parameters

• Formula: C24 H44 Ge4 O4 Te6
• Calculated formula: C24 H44 Ge4 O4 Te6
• SMILES: [Te]1[Ge]2(C(CC(=O)C)(C)C)[Te][Ge](C(CC(=O)C)(C)C)([Te][Ge]3(C(CC(=O)C)(C)C)[Te][Ge]1(C(CC(=O)C)(C)C)[Te]3)[Te]2
• Title of publication: In situ Ge‒Ge bond formation under ambient conditions: synthesis, characterization and reactivity of organo-functionalized telluridogermanate complexes
• Authors of publication: Heimann, Samuel; Holynska, Malgorzata; Dehnen, Stefanie
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2011
• Journal volume: 47
• Journal issue: 6
• Pages of publication: 1881 - 1883
• a: 11.633 ± 0.004 Å
• b: 13.033 ± 0.005 Å
• c: 17.361 ± 0.006 Å
• α: 90°
• β: 131.78 ± 0.05°
• γ: 90°
• Cell volume: 1963 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.136
• Residual factor for significantly intense reflections: 0.1115
• Weighted residual factors for significantly intense reflections: 0.2688
• Weighted residual factors for all reflections included in the refinement: 0.2938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No