Information card for entry 7105922

Structure parameters

• Formula: C12 H20.64 Ge4 O8.3 Te5
• Calculated formula: C12 H20 Ge4 O8.315 Te5
• Title of publication: In situ Ge‒Ge bond formation under ambient conditions: synthesis, characterization and reactivity of organo-functionalized telluridogermanate complexes
• Authors of publication: Heimann, Samuel; Holynska, Malgorzata; Dehnen, Stefanie
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2011
• Journal volume: 47
• Journal issue: 6
• Pages of publication: 1881 - 1883
• a: 10.1 ± 0.003 Å
• b: 50.56 ± 0.01 Å
• c: 12.418 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6341 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 68
• Hermann-Mauguin space group symbol: C c c a :2
• Hall space group symbol: -C 2a 2ac
• Residual factor for all reflections: 0.1265
• Residual factor for significantly intense reflections: 0.0776
• Weighted residual factors for significantly intense reflections: 0.1565
• Weighted residual factors for all reflections included in the refinement: 0.1786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No