Information card for entry 7105923

Structure parameters

• Formula: C28 H36 Ge4 O18 Te5
• Calculated formula: C28 H36 Ge4 O18 Te5
• SMILES: [Te]1[Ge]2([Te][Ge]3([Te][Ge]1([Te][Ge]2([Te]3)C(CC(=O)[O-])CC(=O)[O-])C(CC(=O)[O-])CC(=O)[O-])C(CC(=O)[O-])CC(=O)[O-])C(CC(=O)[O-])CC(=O)[O-].O1CCCC1.O1CCCC1
• Title of publication: In situ Ge‒Ge bond formation under ambient conditions: synthesis, characterization and reactivity of organo-functionalized telluridogermanate complexes
• Authors of publication: Heimann, Samuel; Holynska, Malgorzata; Dehnen, Stefanie
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2011
• Journal volume: 47
• Journal issue: 6
• Pages of publication: 1881 - 1883
• a: 11.901 ± 0.004 Å
• b: 23.406 ± 0.006 Å
• c: 19.298 ± 0.005 Å
• α: 90°
• β: 90.57 ± 0.04°
• γ: 90°
• Cell volume: 5375 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2188
• Residual factor for significantly intense reflections: 0.0603
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 0.643
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No