Information card for entry 7106234

Structure parameters

• Formula: C266 H319 Cl42 Co24 Mo20 O103 P S24
• Calculated formula: C240 H264 Cl6 Co24 Mo19.9984 O95.996 P S24
• Title of publication: p-tert-Butylthiacalix[4]arene-surpported High-nuclearity {Co24M8} (M = Mo or W) Nanospheres and the Hybrids with Keggin Polyoxometalates
• Authors of publication: Yanfeng Bi; Shangchao Du; Wuping Liao
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 4724
• a: 24.6357 ± 0.0003 Å
• b: 24.6357 ± 0.0003 Å
• c: 36.1032 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 21911.7 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0707
• Weighted residual factors for significantly intense reflections: 0.2161
• Weighted residual factors for all reflections included in the refinement: 0.2275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No