Information card for entry 7106235

Structure parameters

• Formula: C250 H287 Cl24 Co24 O100 P S24 W20
• Calculated formula: C240 H264 Cl6 Co24 O96 P S24 W20
• Title of publication: p-tert-Butylthiacalix[4]arene-surpported High-nuclearity {Co24M8} (M = Mo or W) Nanospheres and the Hybrids with Keggin Polyoxometalates
• Authors of publication: Yanfeng Bi; Shangchao Du; Wuping Liao
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 4724
• a: 21.1491 ± 0.0003 Å
• b: 24.093 ± 0.0003 Å
• c: 24.4639 ± 0.0005 Å
• α: 99.761 ± 0.001°
• β: 109.41 ± 0.001°
• γ: 115.439 ± 0.001°
• Cell volume: 9877.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0932
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No