Crystallography Open Database

Information card for entry 7107107

Preview

Coordinates	7107107.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H53 N2 P Pd
Calculated formula	C29 H53 N2 P Pd
SMILES	C1(N(C=CN1C(C)(C)C)C(C)(C)C)=[Pd][P](C1CCCCC1)(C1CCCCC1)C1CCCCC1
Title of publication	Extending unsupported metal-only Lewis pairs to palladium
Authors of publication	Jurgen Bauer; Holger Braunschweig; Alexander Damme; Katrin Gruss; Krzysztof Radacki
Journal of publication	Chem.Commun.
Year of publication	2011
Journal volume	47
Pages of publication	12783
a	9.3082 ± 0.0016 Å
b	9.6832 ± 0.0016 Å
c	18.648 ± 0.003 Å
α	93.263 ± 0.002°
β	93.496 ± 0.002°
γ	118.181 ± 0.002°
Cell volume	1471.8 ± 0.4 Å³
Cell temperature	174 ± 2 K
Ambient diffraction temperature	174 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0339
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0784
Weighted residual factors for all reflections included in the refinement	0.0854
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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