Information card for entry 7107108

Structure parameters

• Formula: C32 H56 Al Cl3 N2 P Pd
• Calculated formula: C32 H56 Al Cl3 N2 P Pd
• Title of publication: Extending unsupported metal-only Lewis pairs to palladium
• Authors of publication: Jurgen Bauer; Holger Braunschweig; Alexander Damme; Katrin Gruss; Krzysztof Radacki
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 12783
• a: 9.3917 ± 0.001 Å
• b: 21.367 ± 0.002 Å
• c: 17.9926 ± 0.0019 Å
• α: 90°
• β: 92.027 ± 0.006°
• γ: 90°
• Cell volume: 3608.4 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0334
• Residual factor for significantly intense reflections: 0.0255
• Weighted residual factors for significantly intense reflections: 0.0618
• Weighted residual factors for all reflections included in the refinement: 0.066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No