Information card for entry 7107428

Structure parameters

• Formula: C52 H70 Ge Mg N4
• Calculated formula: C52 H70 Ge Mg N4
• SMILES: [Ge]1([N](=C(C=C1C(C)(C)C)C(C)(C)C)c1c(cc(cc1C)C)C)N([Mg]1[N](=C(C)C=C(N1c1c(cc(cc1C)C)C)C)c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Contrasting reductions of group 14 metal(II) chloride complexes: synthesis of a ?-diketiminato tin(I) dimer
• Authors of publication: Sam L. Choong; Christian Schenk; Andreas Stasch; Deepak Dange; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2504
• a: 20.546 ± 0.004 Å
• b: 12.171 ± 0.002 Å
• c: 19.87 ± 0.004 Å
• α: 90°
• β: 105.6 ± 0.03°
• γ: 90°
• Cell volume: 4785.8 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1078
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No