Information card for entry 7107429

Structure parameters

• Formula: C64 H96 N4 Pb
• Calculated formula: C64 H96 N4 Pb
• SMILES: [Pb]12([N](=C(C=C(N1c1c(cc(cc1C)C)C)C(C)(C)C)C(C)(C)C)c1c(cc(cc1C)C)C)[N](=C(C=C(N2c1c(cc(cc1C)C)C)C(C)(C)C)C(C)(C)C)c1c(cc(cc1C)C)C.CCCCCC
• Title of publication: Contrasting reductions of group 14 metal(II) chloride complexes: synthesis of a ?-diketiminato tin(I) dimer
• Authors of publication: Sam L. Choong; Christian Schenk; Andreas Stasch; Deepak Dange; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2504
• a: 11.6557 ± 0.0004 Å
• b: 12.1595 ± 0.0004 Å
• c: 22.2271 ± 0.0008 Å
• α: 74.16 ± 0.003°
• β: 76.098 ± 0.003°
• γ: 86.034 ± 0.002°
• Cell volume: 2941.78 ± 0.18 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0842
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No