Information card for entry 7107432

Structure parameters

• Formula: C61 H89 N4 Sn2
• Calculated formula: C61 H89 N4 Sn2
• Title of publication: Contrasting reductions of group 14 metal(II) chloride complexes: synthesis of a ?-diketiminato tin(I) dimer
• Authors of publication: Sam L. Choong; Christian Schenk; Andreas Stasch; Deepak Dange; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2504
• a: 11.094 ± 0.002 Å
• b: 11.584 ± 0.002 Å
• c: 22.708 ± 0.005 Å
• α: 94.78 ± 0.03°
• β: 98.11 ± 0.03°
• γ: 101.14 ± 0.03°
• Cell volume: 2816.2 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.0905
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No