Information card for entry 7107431

Structure parameters

• Formula: C110 H154 Cl4 Mg2 N8 Pb2
• Calculated formula: C110 H154 Cl4 Mg2 N8 Pb2
• Title of publication: Contrasting reductions of group 14 metal(II) chloride complexes: synthesis of a ?-diketiminato tin(I) dimer
• Authors of publication: Sam L. Choong; Christian Schenk; Andreas Stasch; Deepak Dange; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2504
• a: 14.0924 ± 0.0005 Å
• b: 28.9325 ± 0.0009 Å
• c: 27.2581 ± 0.0013 Å
• α: 90°
• β: 95.86 ± 0.004°
• γ: 90°
• Cell volume: 11055.8 ± 0.7 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.114
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.0934
• Weighted residual factors for all reflections included in the refinement: 0.1102
• Goodness-of-fit parameter for all reflections included in the refinement: 0.991
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No