Information card for entry 7107824

Structure parameters

• Formula: C18 H26 N O5 P S Si2 W
• Calculated formula: C18 H26 N O5 P S Si2 W
• Title of publication: The difference between the reactivity of a terminal phosphinidene and a Li/Cl phosphiniodenoid complex in cycloaddition chemistry ‒ in the importance of template-induced selectivity
• Authors of publication: Rainer Streubel; Jose Manuel Villalba Franco; Gregor Schnakenburg; Arturo Espinosa Ferao
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 5986
• a: 9.2854 ± 0.0004 Å
• b: 9.7913 ± 0.0005 Å
• c: 15.3748 ± 0.0007 Å
• α: 72.585 ± 0.002°
• β: 74.551 ± 0.003°
• γ: 77.633 ± 0.003°
• Cell volume: 1271.74 ± 0.11 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0581
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for significantly intense reflections: 0.0779
• Weighted residual factors for all reflections included in the refinement: 0.0832
• Goodness-of-fit parameter for all reflections included in the refinement: 0.951
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No