Information card for entry 7108530

Structure parameters

• Formula: C291.5 H269 Ag20.5 Cl2 F43.5 N84 O48 S14.5
• Calculated formula: C286.5 H260 Ag20.5 Cl2 F28.5 N84 O33 S9.5
• Title of publication: Designed synthesis of a metal cluster-pillared coordination cage
• Authors of publication: Xin He; Cai-Yan Gao; Liang Zhao; Mei-Xiang Wang
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 10877
• a: 35.365 ± 0.007 Å
• b: 21.793 ± 0.004 Å
• c: 50.072 ± 0.01 Å
• α: 90°
• β: 100.51 ± 0.03°
• γ: 90°
• Cell volume: 37944 ± 13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1297
• Residual factor for significantly intense reflections: 0.0919
• Weighted residual factors for significantly intense reflections: 0.2562
• Weighted residual factors for all reflections included in the refinement: 0.282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No