Information card for entry 7108531

Structure parameters

• Formula: C189 H180 Ag15 F27 N48 O30 S9
• Calculated formula: C185 H180 Ag15 F15 N48 O18 S5
• Title of publication: Designed synthesis of a metal cluster-pillared coordination cage
• Authors of publication: Xin He; Cai-Yan Gao; Liang Zhao; Mei-Xiang Wang
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 10877
• a: 22.115 ± 0.003 Å
• b: 22.115 ± 0.003 Å
• c: 178.02 ± 0.04 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 75400 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0835
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1741
• Weighted residual factors for all reflections included in the refinement: 0.1864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No