Information card for entry 7108650

Structure parameters

• Formula: C49 H70 Cl2 Li N7 O Si2 Y2
• Calculated formula: C49 H70 Cl2 Li N7 O Si2 Y2
• Title of publication: Rare-earth metal complexes having an unusual indolyl-1,2-dianion through C‒H activation with a novel η1:(μ2‒η1:η1) bonding with metals
• Authors of publication: Zhu, Xiancui; Zhou, Shuangliu; Wang, Shaowu; Wei, Yun; Zhang, Lijun; Wang, Fenhua; Wang, Shaoyin; Feng, Zhijun
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2012
• Journal volume: 48
• Journal issue: 98
• Pages of publication: 12020 - 12022
• a: 15.0187 ± 0.0013 Å
• b: 16.0047 ± 0.0014 Å
• c: 16.6926 ± 0.0014 Å
• α: 84.159 ± 0.001°
• β: 64.945 ± 0.001°
• γ: 78.9 ± 0.001°
• Cell volume: 3565.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1914
• Residual factor for significantly intense reflections: 0.0888
• Weighted residual factors for significantly intense reflections: 0.2847
• Weighted residual factors for all reflections included in the refinement: 0.3462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No