Crystallography Open Database

Information card for entry 7108705

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Coordinates	7108705.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H56 Ce N4 Si8
Calculated formula	C16 H56 Ce N4 Si8
SMILES	[Ce](N([SiH](C)C)[SiH](C)C)(N([SiH](C)C)[SiH](C)C)(N([SiH](C)C)[SiH](C)C)N([SiH](C)C)[SiH](C)C
Title of publication	A homoleptic tetravalent cerium silylamide
Authors of publication	Alan R. Crozier; Andre M. Bienfait; Cacilia Maichle-Mossmer; Karl W. Tornroos; Reiner Anwander
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	49
Pages of publication	87
a	18.3037 ± 0.0009 Å
b	11.1158 ± 0.0005 Å
c	18.8563 ± 0.0009 Å
α	90°
β	107.559 ± 0.001°
γ	90°
Cell volume	3657.8 ± 0.3 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0279
Residual factor for significantly intense reflections	0.0243
Weighted residual factors for significantly intense reflections	0.0636
Weighted residual factors for all reflections included in the refinement	0.0662
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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