Information card for entry 7110423

Structure parameters

• Formula: C32 H35 F15 N3 O3.5 Sm
• Calculated formula: C32 H27 F15 N3 O3.5 Sm
• Title of publication: Highly electrophilic lanthanide complexes containing fluorinated amido ligands: multiple Ln···F interactions, agostic interactions and η6-arene coordination
• Authors of publication: Click, Damon R.; Scott, Brian L.; Watkin, John G.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 7
• Pages of publication: 633
• a: 10.745 ± 0.001 Å
• b: 10.773 ± 0.001 Å
• c: 18.216 ± 0.002 Å
• α: 98.42 ± 0.01°
• β: 95.81 ± 0.01°
• γ: 114.02 ± 0.01°
• Cell volume: 1874.8 ± 0.4 ų
• Cell temperature: 203 K
• Ambient diffraction temperature: 203 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for all reflections: 0.1218
• Weighted residual factors for significantly intense reflections: 0.1165
• Goodness-of-fit parameter for all reflections: 1.109
• Goodness-of-fit parameter for significantly intense reflections: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No