2,5-Di-(tert-butyl)phospholyl sandwich complexes containing group 14 elements (Ge, Sn, Pb). Synthesis, molecular structure, and ring transfer chemistry of [M(PC4H2But2)2] (M= Sn, Pb)
Authors of publication
Forissier, Kareen; Ricard, Louis; Carmichael, Duncan; Mathey, François
Journal of publication
Chemical Communications
Year of publication
1999
Journal issue
14
Pages of publication
1273
a
16.055 ± 0.0002 Å
b
20.355 ± 0.0004 Å
c
16.491 ± 0.0003 Å
α
90°
β
101.323 ± 0.001°
γ
90°
Cell volume
5284.35 ± 0.16 Å3
Cell temperature
150 ± 0.1 K
Ambient diffraction temperature
150 ± 0.1 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0275
Residual factor for significantly intense reflections
0.0237
Weighted residual factors for significantly intense reflections
0.0622
Weighted residual factors for all reflections included in the refinement
0.0635
Goodness-of-fit parameter for all reflections included in the refinement
