2,5-Di-(tert-butyl)phospholyl sandwich complexes containing group 14 elements (Ge, Sn, Pb). Synthesis, molecular structure, and ring transfer chemistry of [M(PC4H2But2)2] (M= Sn, Pb)
Authors of publication
Forissier, Kareen; Ricard, Louis; Carmichael, Duncan; Mathey, François
Journal of publication
Chemical Communications
Year of publication
1999
Journal issue
14
Pages of publication
1273
a
16.046 ± 0.0002 Å
b
20.328 ± 0.0002 Å
c
16.374 ± 0.0002 Å
α
90°
β
101.089 ± 0.0006°
γ
90°
Cell volume
5241.2 ± 0.11 Å3
Cell temperature
150 ± 0.1 K
Ambient diffraction temperature
150 ± 0.1 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0305
Residual factor for significantly intense reflections
0.0278
Weighted residual factors for significantly intense reflections
0.0737
Weighted residual factors for all reflections included in the refinement
0.0754
Goodness-of-fit parameter for all reflections included in the refinement
