Crystallography Open Database

Information card for entry 7110558

Preview

Coordinates	7110558.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H44 Cl2 O3 Os P2 Sn
Calculated formula	C43 H44 Cl2 O3 Os P2 Sn
Title of publication	Reversible methyl group migration between osmium and tin in reactions of osmium trimethylstannyl complexes
Authors of publication	Rickard, Clifton E. F.; Roper, Warren R.; Woodman, Timothy J.; James Wright, L.
Journal of publication	Chemical Communications
Year of publication	1999
Journal issue	12
Pages of publication	1101
a	9.8497 ± 0.0001 Å
b	11.9753 ± 0.0002 Å
c	18.5656 ± 0.0003 Å
α	95.559 ± 0.001°
β	101.214 ± 0.001°
γ	103.598 ± 0.001°
Cell volume	2064.37 ± 0.05 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0567
Residual factor for significantly intense reflections	0.0401
Weighted residual factors for significantly intense reflections	0.0721
Weighted residual factors for all reflections included in the refinement	0.0809
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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