Information card for entry 7110567

Structure parameters

• Formula: C32 H40 Li2 N2 O2 P2
• Calculated formula: C32 H40 Li2 N2 O2 P2
• Title of publication: Lithiated organophosphorus enamines: a new synthetic approach and the first crystal structures
• Authors of publication: Clegg, William; Liddle, Stephen T.; Davies, Robert P.; Dunbar, Lorraine; Feeder, Neil; Snaith, Ronald; Wheatley, Andrew E. H.; Mulvey, Robert E.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 15
• Pages of publication: 1401
• a: 12.6829 ± 0.0017 Å
• b: 10.2903 ± 0.0014 Å
• c: 24.527 ± 0.003 Å
• α: 90°
• β: 98.782 ± 0.003°
• γ: 90°
• Cell volume: 3163.5 ± 0.7 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.15
• Residual factor for significantly intense reflections: 0.1039
• Weighted residual factors for significantly intense reflections: 0.2926
• Weighted residual factors for all reflections included in the refinement: 0.3095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No