Information card for entry 7110568

Structure parameters

• Formula: C18.88 H22.25 Li N O P
• Calculated formula: C18.78 H21 Li N O P
• Title of publication: Lithiated organophosphorus enamines: a new synthetic approach and the first crystal structures
• Authors of publication: Clegg, William; Liddle, Stephen T.; Davies, Robert P.; Dunbar, Lorraine; Feeder, Neil; Snaith, Ronald; Wheatley, Andrew E. H.; Mulvey, Robert E.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 15
• Pages of publication: 1401
• a: 16.472 ± 0.002 Å
• b: 16.472 ± 0.002 Å
• c: 13.664 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3707.4 ± 1 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 85
• Hermann-Mauguin space group symbol: P 4/n :2
• Hall space group symbol: -P 4a
• Residual factor for all reflections: 0.0858
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for all reflections: 0.2018
• Weighted residual factors for significantly intense reflections: 0.1774
• Goodness-of-fit parameter for all reflections: 1.068
• Goodness-of-fit parameter for significantly intense reflections: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No