Information card for entry 7110983

Structure parameters

• Formula: C9 H20 Cl4 Co2 O3
• Calculated formula: C9 H20 Cl4 Co2 O3
• Title of publication: Unique chains of alternating octahedral and tetrahedral cobalt(ii) sites: crystal structures of the novel chloro-bridged complexes [Co4(μ-Cl)6Cl2(thf)4(MeOH)2]n and [{Co4(μ-Cl)6Cl2(thf)4(H2O)2}·2THF]n
• Authors of publication: Hierso, Jean-Cyrille; Bouwman, Elisabeth; Reedijk, Jan; Ellis, Dianne D.; Spek, Anthony L.
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 15
• Pages of publication: 1359
• a: 10.939 ± 0.0003 Å
• b: 12.151 ± 0.0004 Å
• c: 12.6313 ± 0.0003 Å
• α: 90°
• β: 103.068 ± 0.002°
• γ: 90°
• Cell volume: 1635.47 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0682
• Weighted residual factors for all reflections included in the refinement: 0.0736
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No