Information card for entry 7110984

Structure parameters

• Formula: C12 H26 Cl4 Co2 O4
• Calculated formula: C12 H26 Cl4 Co2 O4
• Title of publication: Unique chains of alternating octahedral and tetrahedral cobalt(ii) sites: crystal structures of the novel chloro-bridged complexes [Co4(μ-Cl)6Cl2(thf)4(MeOH)2]n and [{Co4(μ-Cl)6Cl2(thf)4(H2O)2}·2THF]n
• Authors of publication: Hierso, Jean-Cyrille; Bouwman, Elisabeth; Reedijk, Jan; Ellis, Dianne D.; Spek, Anthony L.
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 15
• Pages of publication: 1359
• a: 8.6714 ± 0.0003 Å
• b: 10.8418 ± 0.0003 Å
• c: 11.8514 ± 0.0005 Å
• α: 76.563 ± 0.002°
• β: 77.804 ± 0.002°
• γ: 68.245 ± 0.002°
• Cell volume: 996.81 ± 0.06 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0651
• Weighted residual factors for all reflections included in the refinement: 0.0699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No