Information card for entry 7111848

Structure parameters

• Formula: C41 H46 Cl O P2 Rh
• Calculated formula: C41 H46 Cl O P2 Rh
• Title of publication: A simple route to azaborinylphosphines: isoelectronic B-N analogues of arylphosphine ligands
• Authors of publication: Jonathan A. Bailey; Mairi F. Haddow; Paul G. Pringle
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 1432
• a: 9.73 ± 0.0003 Å
• b: 23.1553 ± 0.0008 Å
• c: 8.03 ± 0.0003 Å
• α: 90°
• β: 103.596 ± 0.002°
• γ: 90°
• Cell volume: 1758.47 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0902
• Weighted residual factors for all reflections included in the refinement: 0.1063
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No