Information card for entry 7111849

Structure parameters

• Formula: C47 H50 Cl5 O P2 Rh
• Calculated formula: C47 H50 Cl5 O P2 Rh
• Title of publication: A simple route to azaborinylphosphines: isoelectronic B-N analogues of arylphosphine ligands
• Authors of publication: Jonathan A. Bailey; Mairi F. Haddow; Paul G. Pringle
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 1432
• a: 8.5503 ± 0.0005 Å
• b: 11.5693 ± 0.0007 Å
• c: 11.8543 ± 0.0007 Å
• α: 69.3 ± 0.003°
• β: 84.914 ± 0.003°
• γ: 72.868 ± 0.003°
• Cell volume: 1048.11 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0172
• Residual factor for significantly intense reflections: 0.0169
• Weighted residual factors for significantly intense reflections: 0.045
• Weighted residual factors for all reflections included in the refinement: 0.0452
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No