Information card for entry 7112797

Structure parameters

• Formula: C32 H54 Cl2 Li2 N8 Y2
• Calculated formula: C32 H54 Cl2 Li2 N8 Y2
• SMILES: [Y]12345678([cH]9[cH]7[cH]6[cH]5[cH]49)[N]4(C)[CH]52[N]1(CCC4)C[N]12[Li]45([N]([CH]314)(CCC2)C)[Cl][Y]1234567([cH]9[cH]7[cH]6[cH]5[cH]49)[N]4(C)[CH]52[N]1(CCC4)C[N]12[Li]45([N]([CH]314)(CCC2)C)[Cl]8
• Title of publication: Three different product types from reactions of lithiated cyclic aminals with trivalent organometal chlorides.
• Authors of publication: Hellmann, Benjamin J.; Kamps, Ina; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 35
• Pages of publication: 6536 - 6538
• a: 8.477 ± 0.0001 Å
• b: 21.3447 ± 0.0004 Å
• c: 10.8024 ± 0.0002 Å
• α: 90°
• β: 105.85 ± 0.0011°
• γ: 90°
• Cell volume: 1880.26 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0241
• Weighted residual factors for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.0588
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No