Information card for entry 7112798

Structure parameters

• Formula: C21.5 H33 N4 Y
• Calculated formula: C18 H29.5 N4 Y
• Title of publication: Three different product types from reactions of lithiated cyclic aminals with trivalent organometal chlorides.
• Authors of publication: Hellmann, Benjamin J.; Kamps, Ina; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 35
• Pages of publication: 6536 - 6538
• a: 25.8849 ± 0.0019 Å
• b: 12.5835 ± 0.0009 Å
• c: 17.2346 ± 0.0013 Å
• α: 90°
• β: 129.264 ± 0.003°
• γ: 90°
• Cell volume: 4346.3 ± 0.6 ų
• Cell temperature: 225 ± 2 K
• Ambient diffraction temperature: 225 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0272
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0727
• Weighted residual factors for all reflections included in the refinement: 0.0735
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No