Information card for entry 7112963

Structure parameters

• Formula: C23 H25 N3 Pd
• Calculated formula: C23 H25 N3 Pd
• Title of publication: Unusual transmetallation-induced formation of a C2-symmetric tetrapallada-macrocycle.
• Authors of publication: Annibale, Vincent T.; Lund, Liisa M.; Song, Datong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 43
• Pages of publication: 8261 - 8263
• a: 11.1137 ± 0.0006 Å
• b: 23.4596 ± 0.0015 Å
• c: 11.9041 ± 0.0006 Å
• α: 90°
• β: 98.157 ± 0.002°
• γ: 90°
• Cell volume: 3072.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections included in the refinement: 0.0967
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No