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Information card for entry 7112964
Preview
Coordinates | 7112964.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H44 Cl4 N4 Pd4 |
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Calculated formula | C46 H44 Cl4 N4 Pd4 |
SMILES | CC1C2C(C)=[N]([Pd]3([N]=1c1ccccc1)[Cl][Pd](C1C(C)=[N](c4ccccc4)[Pd]4([N](=C1C)c1ccccc1)[Cl][Pd]2(c1ccccc1)[Cl]4)(c1ccccc1)[Cl]3)c1ccccc1 |
Title of publication | Unusual transmetallation-induced formation of a C2-symmetric tetrapallada-macrocycle. |
Authors of publication | Annibale, Vincent T.; Lund, Liisa M.; Song, Datong |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2010 |
Journal volume | 46 |
Journal issue | 43 |
Pages of publication | 8261 - 8263 |
a | 21.5383 ± 0.0008 Å |
b | 13.627 ± 0.0003 Å |
c | 18.8184 ± 0.0006 Å |
α | 90° |
β | 124.523 ± 0.0011° |
γ | 90° |
Cell volume | 4550.6 ± 0.3 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0439 |
Residual factor for significantly intense reflections | 0.0334 |
Weighted residual factors for significantly intense reflections | 0.0826 |
Weighted residual factors for all reflections included in the refinement | 0.0881 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7112964.html
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