Information card for entry 7112965

Structure parameters

• Formula: C38 H42 Br2 Cl8 N4 Pd2
• Calculated formula: C38 H42 Br2 Cl8 N4 Pd2
• Title of publication: Unusual transmetallation-induced formation of a C2-symmetric tetrapallada-macrocycle.
• Authors of publication: Annibale, Vincent T.; Lund, Liisa M.; Song, Datong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 43
• Pages of publication: 8261 - 8263
• a: 8.8468 ± 0.0002 Å
• b: 23.2955 ± 0.0007 Å
• c: 11.6038 ± 0.0003 Å
• α: 90°
• β: 110.589 ± 0.0013°
• γ: 90°
• Cell volume: 2238.69 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0547
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.0992
• Weighted residual factors for all reflections included in the refinement: 0.1064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No