Crystallography Open Database

Information card for entry 7113243

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Coordinates	7113243.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H99 N2 P Pb Si2
Calculated formula	C63 H99 N2 P Pb Si2
Title of publication	A new type of heteroleptic complex of divalent lead and synthesis of the P-plumbyleniophosphasilene, R2Si=P‒Pb(L): (L = β-diketiminate)
Authors of publication	Yao, Shenglai; Block, Stefan; Brym, Markus; Driess, Matthias
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2007
Journal issue	37
Pages of publication	3844 - 3846
a	12.4953 ± 0.0002 Å
b	18.9054 ± 0.0003 Å
c	14.3412 ± 0.0002 Å
α	90°
β	109.26 ± 0.0017°
γ	90°
Cell volume	3198.18 ± 0.09 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0301
Residual factor for significantly intense reflections	0.0219
Weighted residual factors for significantly intense reflections	0.0558
Weighted residual factors for all reflections included in the refinement	0.0616
Goodness-of-fit parameter for all reflections included in the refinement	1.191
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7102149
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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