Information card for entry 7113372

Structure parameters

• Formula: C56 H42 B F24 Fe2 Ga O4
• Calculated formula: C56 H42 B F24 Fe2 Ga O4
• Title of publication: Fe-Ga multiple bonding? Synthesis, spectroscopic and structural characterization of a transition metal complex containing a cationic two-coordinate gallium centre.
• Authors of publication: Bunn, Natalie R.; Aldridge, Simon; Coombs, Deborah L.; Rossin, Andrea; Willock, David J.; Jones, Cameron; Ooi, Li-ling
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 15
• Pages of publication: 1732 - 1733
• a: 14.442 ± 0.003 Å
• b: 15.004 ± 0.003 Å
• c: 15.541 ± 0.003 Å
• α: 66.25 ± 0.03°
• β: 71.75 ± 0.03°
• γ: 75.17 ± 0.03°
• Cell volume: 2894.5 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0599
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1038
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No