Information card for entry 7113373

Structure parameters

• Formula: C48 H32 Cl F9 N3 P2 Ru Sb
• Calculated formula: C48 H32 Cl F9 N3 P2 Ru Sb
• Title of publication: A new class of tethered-arene ruthenium(II) complexes with pendant P and C donor atoms: synthesis of eta6:eta1:eta1 phosphonio-azabutadienyl ruthenabicycles via allenylidene intermediates.
• Authors of publication: Cadierno, Victorio; Díez, Josefina; García-Alvarez, Joaquín; Gimeno, José
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 16
• Pages of publication: 1820 - 1821
• a: 39.587 ± 0.007 Å
• b: 12.43 ± 0.002 Å
• c: 20.522 ± 0.004 Å
• α: 90°
• β: 117.306 ± 0.007°
• γ: 90°
• Cell volume: 8973 ± 3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1175
• Residual factor for significantly intense reflections: 0.0603
• Weighted residual factors for significantly intense reflections: 0.1392
• Weighted residual factors for all reflections included in the refinement: 0.1652
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No