Information card for entry 7113374

Structure parameters

• Formula: C54 H44 Cl F10 N2 P2 Ru Sb
• Calculated formula: C54 H44 Cl F10 N2 P2 Ru Sb
• Title of publication: A new class of tethered-arene ruthenium(II) complexes with pendant P and C donor atoms: synthesis of eta6:eta1:eta1 phosphonio-azabutadienyl ruthenabicycles via allenylidene intermediates.
• Authors of publication: Cadierno, Victorio; Díez, Josefina; García-Alvarez, Joaquín; Gimeno, José
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 16
• Pages of publication: 1820 - 1821
• a: 16.4727 ± 0.0016 Å
• b: 17.1842 ± 0.0017 Å
• c: 20.571 ± 0.002 Å
• α: 90°
• β: 112.879 ± 0.002°
• γ: 90°
• Cell volume: 5364.9 ± 0.9 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.1988
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1733
• Weighted residual factors for all reflections included in the refinement: 0.2328
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No