Information card for entry 7113817

Structure parameters

• Formula: C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4
• Calculated formula: C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4
• Title of publication: Synthesis and luminescence behaviour of novel heterodecanuclear silver(I)–rhenium(I) alkynyl complexes. X-Ray crystal structures of [Ag6(μ-dppm)4{μ3-C≡CC≡C–Re(Me2bpy)(CO)3}4](PF6)2 and [Ag6(μ-dppm)4{μ3-C≡CC≡C–Re(Br2phen)(CO)3}4](PF6)2
• Authors of publication: Yam, Vivian Wing-Wah; Lo, Wing-Yin; Zhu, Nianyong
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 19
• Pages of publication: 2446 - 2447
• a: 27.379 ± 0.004 Å
• b: 27.379 ± 0.004 Å
• c: 16.984 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12731 ± 3 ų
• Cell temperature: 253 ± 2 K
• Ambient diffraction temperature: 253 ± 2 K
• Number of distinct elements: 9
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.1023
• Residual factor for significantly intense reflections: 0.0665
• Weighted residual factors for significantly intense reflections: 0.2207
• Weighted residual factors for all reflections included in the refinement: 0.2395
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No