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Information card for entry 7113817
Preview
Coordinates | 7113817.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4 |
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Calculated formula | C176 H112 Ag6 Br8 F12 N8 O12 P10 Re4 |
Title of publication | Synthesis and luminescence behaviour of novel heterodecanuclear silver(i)?rhenium(i) alkynyl complexes. X-Ray crystal structures of [Ag6(�-dppm)4{�3-C?CC?C?Re(Me2bpy)(CO)3}4](PF6)2 and [Ag6(�-dppm)4{�3-C?CC?C?Re(Br2phen)(CO)3}4](PF6)2Electronic supplementary information (ESI) available: characterisation for 1?4, perspective drawing of the complex cation of 4, and detailed X-ray crystal structure determination data for 2 and 4. See http://www.rsc.org/suppdata/cc/b3/b307479j/ |
Authors of publication | Yam, Vivian Wing-Wah; Lo, Wing-Yin; Zhu, Nianyong |
Journal of publication | Chemical Communications |
Year of publication | 2003 |
Journal issue | 19 |
Pages of publication | 2446 |
a | 27.379 ± 0.004 Å |
b | 27.379 ± 0.004 Å |
c | 16.984 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 12731 ± 3 Å3 |
Cell temperature | 253 ± 2 K |
Ambient diffraction temperature | 253 ± 2 K |
Number of distinct elements | 9 |
Space group number | 86 |
Hermann-Mauguin space group symbol | P 42/n :2 |
Hall space group symbol | -P 4bc |
Residual factor for all reflections | 0.1023 |
Residual factor for significantly intense reflections | 0.0665 |
Weighted residual factors for significantly intense reflections | 0.2207 |
Weighted residual factors for all reflections included in the refinement | 0.2395 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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