Information card for entry 7114559

Structure parameters

• Formula: C51 H69 N3 U
• Calculated formula: C51 H69 N3 U
• SMILES: [U]12345678(=NN=C(c9ccccc9)c9ccccc9)(=Nc9c(cc(cc9C(C)(C)C)C(C)(C)C)C(C)(C)C)([c]9([c]1([c]2([c]3([c]49C)C)C)C)C)[c]1([c]5([c]6([c]7([c]81C)C)C)C)C
• Title of publication: Enhancing the reactivity of uranium(vi) organoimido complexes with diazoalkanesElectronic supplementary information (ESI) available: experimental, including general procedures, materials and synthesis of complexes 2 and 3. See http://www.rsc.org/suppdata/cc/b1/b109455f/
• Authors of publication: Kiplinger, Jaqueline L.; Morris, David E.; Scott, Brian L.; Burns, Carol J.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 1
• Pages of publication: 30
• a: 12.407 ± 0.004 Å
• b: 29.634 ± 0.007 Å
• c: 12.836 ± 0.004 Å
• α: 90°
• β: 103.484 ± 0.005°
• γ: 90°
• Cell volume: 4589 ± 2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0872
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.233
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No