Information card for entry 7114560

Structure parameters

• Formula: C54 H75 N3 U
• Calculated formula: C54 H68 N3 U
• Title of publication: Enhancing the reactivity of uranium(vi) organoimido complexes with diazoalkanesElectronic supplementary information (ESI) available: experimental, including general procedures, materials and synthesis of complexes 2 and 3. See http://www.rsc.org/suppdata/cc/b1/b109455f/
• Authors of publication: Kiplinger, Jaqueline L.; Morris, David E.; Scott, Brian L.; Burns, Carol J.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 1
• Pages of publication: 30
• a: 10.778 ± 0.003 Å
• b: 21.982 ± 0.007 Å
• c: 22.876 ± 0.009 Å
• α: 104.703 ± 0.009°
• β: 98.253 ± 0.006°
• γ: 102.868 ± 0.007°
• Cell volume: 4994 ± 3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1247
• Residual factor for significantly intense reflections: 0.0951
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1176
• Goodness-of-fit parameter for all reflections included in the refinement: 2.314
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No